The Elegra Argon Humidifier

Uninterrupted and Maintenance-Free ICP Operation

The Elegra Argon Humidifier is commonly used in ICP analyses involving samples with high concentrations of dissolved solids. It helps to alleviate salt deposits in the nebulizer and torch injector, allowing uninterrupted and maintenance-free operation.

Elegra Hero

Uninterrupted and Maintenance-Free ICP Operation

It is standard practice to use dry argon for the nebulizer gas in ICP to generate an aerosol and transport the sample to the plasma. However, with samples containing high amounts of total dissolved solids (TDS) there is an increased likelihood of salt deposits forming at the tip of the nebulizer and injector which can result in significant analytical drift in or even an extinguished plasma. To successfully measure challenging sample matrices with high TDS, it is important to optimize your ICP sample introduction system including a:

  • Suitable, high TDS nebulizer (e.g. SeaSpray™ or DuraMist™)
  • Double-pass, cyclonic spray chamber to filter out large droplets (e.g. Twister™)
  • Wide bore injector (2.0mm ID or greater)
  • Humidified argon nebulizer gas supply

Adding an argon humidifier such as the Elegra, will reduce maintenance and the chance of an extinguished plasma owing to a blocked nebulizer or injector.

Long-term stability test
Figure 1. Long-term stability test, 4 hour analysis of 1pmm standard in 10.0 % NaCl

Design

The elegant design of the Elegra is compact and made of inert, metal-free materials so it is easier to fit into the often crowded, harsh environment of the sample compartment of any ICP.

The novel, highly efficient membrane technology adds moisture to the argon nebulizer gas without the need for pressurization or electrical heating. The Elegra can be configured as either a:

  • Single-channel version with a bypass switch to turn humidification on and off
  • Dual-channel version for simultaneously humidifying the nebulizer gas and auxiliary/dilution gases often used in ICP-MS

The Elegra is available in range of configurations with customized gas connectors to exactly suit your ICP.

Elegra and Elegra Dual
Figure 2. Elegra Argon Humidifier & Elegra Dual Argon Humidifer

Easy Installation

For easy and straight forward installation on any ICP instrument and with any nebulizer, each Elegra Kit is packaged with customized gas connectors to exactly suit your ICP. A detailed assembly guide is also included.

Elegra Installation on Thermo PRO
Figure 3. Elegra Installation on Thermo Scientific™ PRO ICP-OES (P/N 70-803-1303)

Superior Performance

The relative humidity (RH) added by the Argon humidifier will determine the efficiency and overall performance as to how well the accessory can slow and prevent salt build-up at the nebulizer and injector. As a comparison of humidification efficiency, the RH output of the Elegra was compared to another commercially available argon humidifier that requires a power supply and heating element, which is referred to as Brand-X. The Brand-X model was specifically selected in this comparison as it is listed as the supplier’s “enhanced humidification model.”

At an argon gas flow rate of 0.7 L/min and in heated mode, Brand-X is 25% less effective compared to the Elegra, which requires no power supply, electrical cords, or added heat. With no added heat, at room temperature Brand-X produced 60% less RH on average compared to the Elegra.

Percent Humidity
Figure 4. Percent Humidity Relative to Elegra (Elegra = 1)

The nebulizer is a critical component of your ICP sample introduction system, so why not opt for the highest quality? Glass Expansion has been manufacturing ICP nebulizers since the early 1980s and continually updates nebulizer designs to improve performance and ease of use. Whether your ICP laboratory is analyzing clean aqueous samples, samples containing HF and/or high dissolved salts, or volatile organic solvents; Glass Expansion has a nebulizer to suit your needs.

Internal standard stability
Figure 5. Internal standard stability in 0.5% lithium metaborate/tetraborate with Elegra Ar humidifier
Internal standard stability
Figure 6. Internal standard stability in 0.5% lithium metaborate/tetraborate without Elegra Ar humidifier

For those customers familiar with Glass Expansion’s original humidifier design, the Capricorn™, you can rest assured that the Elegra is an upgraded design with equivalent RH performance. Two Capricorn units, labeled A and B, were compared to two Elegra units, also labeled A and B, to ensure that the Elegra was an equivalent replacement to the original humidifier design. After 5 minutes, both the Elegra and Capricorn average out to a stable RH of approximately 92%.

Elegra and Capricorn Humidifier Comparison
Figure 7. Elegra and Capricorn Humidifier % RH Comparison

Ordering Information

Elegra Single-Channel Argon Humidifier Kits

Part Number To Suit
70-803-1265 Agilent®, Varian Vista, 700-ES, MP-AES
70-803-1268 Agilent® 5100, 5110, 5800, 5900
70-803-1268 Agilent® 7700, 7800, 7850, 7900, 8800, 8900
70-803-1266 Horiba® Jobin Yvon
70-803-1265 Teledyne™ Leeman
70-803-1269 PerkinElmer® AVIO, Optima
70-803-1270 PerkinElmer® Elan/NexION 300 Series
70-803-1312 Shimadzu® ICP-OES 7000, 8000, 9000, 9800 Series / ICPM-8500, ICPMS-2030
70-803-1269 Spectro™
70-803-1268 Thermo Scientific™ PRO, 6000/7000, Q/RQ/TQ, X Series
70-803-1271 Other models (Universal Kit)
70-803-1581 Elegra Mount

Elegra Dual-Channel Argon Humidifier Kits

Part Number To Suit
70-803-1273 Agilent® 7700, 7800, 7850, 7900, 8800, 8900
70-803-1274 PerkinElmer® Elan/NexION 300 Series
70-803-1473 PerkinElmer® Nexion 1000, 1100, 2000, 2200, 5000 Series
70-803-1273 Thermo Scientific™ Q, RQ, TQ
70-803-1273 Other models (Universal Kit)
70-803-1581 Elegra Mount

Customer Comments

We installed and ran samples with the argon humidifier into both the Thermo Scientific™ 7000 ICP, as well as our ICPMS. We noticed that the iCAP™ ICP could handle TCLP samples which have a very high sodium matrix much better. Typically, the carrier gas pressure would creep up from 250 to 450 and we'd have to clean the nebulizer after 1 run of TCLP samples. Now, the carrier gas pressure stays low for longer. Fantastic!

The (Elegra) Humidifier (and adjusting our pump speed) really helped to stabilize the drift we were previously experiencing between QC checks and especially helped combat some of our high TDS samples. Our runs have greatly improved.

(In reference to the Elegra) Talking with my operators that are here today neither of them has changed a nebulizer since we put it https://on........we/ had been replacing nebulizers after about a week and half........I will be ordering 2 more.

I'm very happy with the performance of the Elegra so far. It's been in use since Sep 14th and we haven't had to change or clean the neb once.

For all enquiries or more information:

Contact Glass Expansion